›› 2013, Vol. 4 ›› Issue (3): 134-137.

• 论著 • 上一篇    下一篇

表面不同形貌对钛耐腐蚀性能影响的实验研究

聂鹤鹏1,王国平2,王培志2,邱憬2   

  1. 1. 南京医科大学附属口腔医院
    2. 南京医科大学附属口腔医院种植修复科
  • 收稿日期:2013-05-28 修回日期:2013-09-13 出版日期:2013-09-25 发布日期:2013-10-22
  • 通讯作者: 聂鹤鹏 E-mail:arthur1487511@sina.com

Corrosion resistance research on pure titanium with different roughness of the surface

  1. 1. 南京医科大学附属口腔医院
    2. Department of Implantology,Affiliated Hospital of Stomatology, Nanjing Medical University
  • Received:2013-05-28 Revised:2013-09-13 Online:2013-09-25 Published:2013-10-22
  • Contact: 王国平 E-mail:arthur1487511@sina.com

摘要: 目的:评价方法不同表面处理后纯钛表面粗糙程度对其耐腐蚀性能的影响。方法:纯钛试件制备33个并随机分为三组,分别进行喷砂,阳极氧化和机械抛光处理,应用扫描电镜观察不同处理后钛件表面微形貌,在酸性含氟人工唾液中测试开路电位和阳极极化曲线。结果:扫描电镜结果显示喷砂后表面大量的弹坑和划痕,深度较深,且形状不规则,大小不一,边缘锐利,为微米级粗糙表面形态;而阳极氧化表面为大小均一的直径80nm的纳米管状结构,为纳米级粗糙表面形态;机械抛光表面划痕明显,深度较浅,为微米级粗糙表面形态。在酸性含氟人工唾液中,三组之间自腐蚀电位为阳极氧化组>机械抛光组>喷砂组,腐蚀电流喷砂组>机械抛光组>阳极氧化组,具有显著性差异。结论:纯钛试件表面经过不同表面处理后的耐腐蚀性为阳极氧化组>机械抛光组>喷砂组。

Abstract: Objective: To evaluate the corrosion resistance of different roughness surface of the titanium after different surface treatment. Methods: Thirty-three pure titanium specimens were cast and divided into three groups randomly, and then were treated by sandblasting, anodic oxidation and mechanical polishing separately. SEM was thereafter used to observed the surface of titanium after modification. Open circle potential and anode polarization curve were determined in acid artificial saliva containing fluoride. Results: SEM results showed that the surface of titanium after sandblasting exhibited micro-topographical massive deep scratches and pits of irregular shape, different size and sharp edge. But on the anodic oxidation surface nanotopographic, 80 nm-diameter nanotubes were formed. The surface of titanium after mechanical polishing had micro-topographic shallow scratches. In the acid artificial saliva,the corrosion potentials of three groups were in the sequence of anodic oxidation group>mechanical polished group>sandblasted group. The corrosion currents of three groups were sandblasted group>mechanical polished group>anodic oxidation group. Both data have statistical significance. Conclusions: Different surface modifications changed the topography of the titanium and affected the titanium’s corrosion resistance. The nanotopograhpy of titanium achieved by anodic oxidation had better corrosion resistance and sandblasting reduced the corrosion resistance of titanium

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